Fsdss673 Hot Access

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3.2. High‑Temperature Structural Evolution

| Temperature (°C) | Observed Phase | Lattice Parameters | ΔV/V (%) | |------------------|----------------|--------------------|----------| | 25 – 600 | α‑FSDSS673 | a = …, c = … | – | | 600 – 800 | Onset of transition (peak broadening) | – | +0.3 | | 800 – 950 | β‑FSDSS673 (new peaks at 2θ ≈ … ) | a = …, c = … | +1.2 | | > 950 | Re‑recrystallisation to α‑phase (cooling) | – | – | fsdss673 hot

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